Definition
Moisture Analyzer is the instrument that measures water content of resin before processing, verifying that drying was sufficient. It is the last line of defense against moisture defects: splay, bubbles, hydrolysis (chemical degradation) and unstable dimensions.
Measurement principles
- Loss On Drying (LOD): heats the sample to constant weight. Inexpensive, slow (15 – 30 min)
- Karl Fischer: chemical titration with water-specific reagent. Very precise (±10 ppm). Reference standard.
- Coulometric: automated Karl Fischer variant, fast (3 – 8 min)
- Capacitive / dielectric: in-line, continuously monitors moisture in the drying hopper
Typical maximum levels
- PA 6 / PA 66: <0.15 – 0.20 %
- PC: <0.02 %
- PET: <0.005 % (50 ppm)
- ABS: <0.10 %
- PBT: <0.04 %
- PP, PE: no routine measurement needed (non-hygroscopic)
Ideal shop-floor procedure
- Sample from the hopper just above the feed throat
- Sample size: 5 – 10 g
- Measure with Karl Fischer (lab) or LOD analyzer (production)
- Log each batch in the process record
- Frequency: at every material change and once per shift
Commercial equipment
- Karl Fischer: Metrohm, Mettler Toledo
- Compact LOD: Sartorius, A&D, OHAUS
- In-line (dielectric): Process Sensors, Aboniq
Common mistakes
Calibration not verified with a standard sample, oven contamination (previous residues), inadequate sample size, and not purging the sampling line before drawing (ambient moisture).
Synonyms